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国家自然科学基金(51231005)

作品数:8 被引量:22H指数:2
相关作者:付琴琴单智伟田琳张朋诚更多>>
相关机构:西安交通大学更多>>
发文基金:国家自然科学基金国家重点基础研究发展计划高等学校学科创新引智计划更多>>
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An index for deformation controllability of small-volume materials
2014年
Mechanical tests on small-volume materials show that in addition to the usual attributes of strength and ductility, the controlla- bility of deformation would be crucial for the purpose of precise plastic shaping. In our present work, a "mechanical controlla- bility index" (MCI) has been proposed to assess the controllability of mechanical deformation quantitatively. The index allows quantitative evaluation of the relative fraction of the controllable plastic strain out of the total strain. MCI=0 means completely uncontrollable plastic deformation, MCI=∞ means perfectly controllable plastic shaping. The application of the index is demonstrated here by comparing two example cases: 0.273 to 0.429 for single crystal A1 nanopillars that exhibit obvious strain bursts, versus 3.17 to 4.2 for polycrystalline A1 nanopillars of similar size for which the stress-strain curve is smoother.
WANG ZhangJieSHAN ZhiWeiLI JuSUN JunMA Evan
聚焦离子束在微纳尺度材料力学性能研究中的应用被引量:3
2013年
微纳尺度材料是指外观尺寸或其基本构成单元在10 nm到10μm之间(以下简称微纳尺度)的材料或器件。个案、定性的研究表明微纳尺度材料有以下特性:其性能不能通过外推基于宏观块体材料的知识体系得到,传统的力学测试工具和方法无法满足对微纳尺度材料进行测试的要求,微纳尺度材料通常在多场耦合条件下服役。这些特性要求研究工作者持续不断地寻找和研发新的工具以期实现对微纳尺度材料的可控制备,高通量观测、操控和定量测量。双束聚焦离子束技术不仅因具有纳米级的空间分辨率而具备对微纳尺度材料的高质量成像和动态监测,而且具备纳米分辨率的定点刻蚀、诱导沉积等功能。因此,双束聚焦离子束成为研究微纳尺度材料力学性能的有力工具。综述了近年来聚焦离子束技术在微纳尺度材料类力学性能研究中的应用,并讨论了其局限性和发展趋势。
田琳付琴琴单智伟
关键词:聚焦离子束
Ultrafast shape change and joining of small-volume materials using nanoscale electrical discharge
2015年
Using nanoscale electrical-discharge-induced rapid Joule heating, we developed a method for ultrafast shape change and joining of small-volume materials. Shape change is dominated by surface-tension-driven convection in the transient liquid melt, giving an extremely high strain rate of N106 s-1. In addition, the heat can be dissipated in small volumes within a few microseconds through thermal conduction, quenching the melt back to the solid state with cooling rates up to 108 K.s-1. We demonstrate that this approach can be utilized for the ultrafast welding of small-volume crystalline Mo (a refractory metal) and amorphous Cu49Zr51 without introducing obvious microstructural changes, distinguishing the process from bulk welding.
Cheng-Cai WangQing-Jie LiLiang ChenYong-Hong ChengJun SunZhioWei ShanJu LiEvan Ma
关键词:METALLIC
FIB-SEM双束技术简介及其部分应用介绍被引量:19
2016年
聚焦离子束(FIB)与扫描电子显微镜(SEM)耦合成为FIB-SEM双束系统后,通过结合相应的气体沉积装置,纳米操纵仪,各种探测器及可控的样品台等附件成为一个集微区成像、加工、分析、操纵于一体的分析仪器。其应用范围也已经从半导体行业拓展至材料科学、生命科学和地质学等众多领域。本文介绍了双束系统中的一些关键概念及基本原理并综述了其在材料科学领域的一些典型应用,包括透射电镜(TEM)样品制备,微纳尺度力学测试样品制备以及材料三维成像及分析。
付琴琴单智伟
一种基于聚焦离子束技术的环境透射电镜光阑清理方法被引量:1
2016年
光阑是透射电子显微镜电子光学系统的重要部件之一,其对透射电镜的成像质量有着重要的影响,然而原位环境透射电镜由于在使用中经常需要通入气氛并配合加热,因污染累积导致光阑的使用寿命大为降低。本文针对传统真空高温灼烧清理光阑方法需要较强的经验性及成功率低的缺点,提出一种新的光阑清理方法。该方法使用聚焦离子束(FIB)可定点、高效地清理光阑孔边缘的各种污染物,在恢复光阑孔圆度的同时又不会对光阑的其他部分造成损伤而引起失效。最终测试结果表明清理后的光阑满足透射电镜的使用要求,因此这种基于FIB技术的加工手段为电镜工作者提供了一种高效、精确和无损的光阑清理方法。
付琴琴张朋诚单智伟
关键词:光阑聚焦离子束透射电子显微镜
Unit-cell-reconstruction:A novel plastic deformation mechanism discovered in magnesium
2015年
Prof.Shan Zhiwei’s group at Xi’an Jiaotong University discovered a novel mechanism for room temperature plastic deformation in magnesium(Nature Communications,2014,5:3297).Magnesium and its alloys have been intensively studied for several decades due to their potential applications in automobile and aerospace industry.Deformation twinning and dislocation slip are known to be
关键词:MAGNESIUMDISLOCATIONFIGUREBASALDEFORMED
Insight from in situ microscopy into which precipitate morphology can enable high strength in magnesium alloys
2018年
Magnesium alloys, while boasting light weight, suffer from a major drawback in their relatively low strength. Identifying the microstructural features that are most effective in strengthening is therefore a pressing challenge. Deformation twinning often mediates plastic yielding in magnesium alloys. Unfortunately, due to the complexity involved in the twinning mechanism and twin-precipitate interactions, the optimal precipitate morphology that can best impede twinning has yet to be singled out. Based on the understanding of twinning mechanism in magnesium alloys, here we propose that the lamellar precipitates or the network of plate-shaped precipitates are most effective in suppressing deformation twinning. This has been verified through quantitative in situ tests inside a transmission electron microscope on a series of magnesium alloys containing precipitates with different morphology. The insight gained is expected to have general implications for strengthening strategies and alloy design. 2018 Published by Elsevier Ltd on behalf of The editorial office of Journal of Materials Science & Technology.
Bo-Yu LiuNan YangJian WangMatthew BarnettYun-Chang XinDi WuRen-Long XinBin LiR. Lakshmi NarayanJian-Feng NieJu LiEvan MaZhi-Wei Shan
纯铁的理论剪切强度获得实验证实
2015年
金属的理论强度是指其晶体点阵失稳前所能承受的最大应力。金属材料的实际强度大大低于其理论强度,主要原因在于实际的材料中存在大量的缺陷,而缺陷可以使材料通过局部滑移等方式发生塑性变形,所需外力显著降低。近年来科学家所关注的'越小越强'效应,也就是说微纳尺度金属样品的强度会随着样品尺寸的减小而提高的现象,原因之一就在于小样品中的晶体缺陷更少。即便如此。
郑雁军
关键词:金属材料晶体缺陷剪切强度纳米铁
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